3α-Acetyloxy-5α-pregnan-20-one synthesis
- Product Name:3α-Acetyloxy-5α-pregnan-20-one
- CAS Number:1491-77-6
- Molecular formula:C23H36O3
- Molecular Weight:360.5302
4057-84-5
23 suppliers
inquiry
1491-77-6
7 suppliers
$875.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 63 percent / Pb(OAc)4, Cu(OAc)2, pyridine / benzene / 4 h / Heating
2: 90 percent / Li/ethylenediamine / 0.25 h / Heating
3: pyridine / 18 h / Ambient temperature
4: 1.) O3, 2.) Jones reagent / 1.) CH2Cl2, -10 deg C, 2.) acetone, 0 deg C
References:
Deluca;Seldes;Garraffo;Gros [Zeitschrift fur Naturforschung, Teil B: Anorganische Chemie, Organische Chemie,1984,vol. 39,# 11,p. 1617 - 1621]
50630-72-3
1 suppliers
inquiry
1491-77-6
7 suppliers
$875.00/100mg