3-AMINO-N-BENZYL-N-METHYLBENZAMIDE synthesis
- Product Name:3-AMINO-N-BENZYL-N-METHYLBENZAMIDE
- CAS Number:865610-58-8
- Molecular formula:C15H16N2O
- Molecular Weight:240.3
195140-22-8
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Yield:865610-58-8 95%
Reaction Conditions:
with tin(ll) chloride in ethyl acetate at 20; for 3 h;
Steps:
111.b
To a solution of N-benzyl-N-methyl-3-nitro-benzamide (320mg, l.lδmmol) in ethyl acetate (10ml) was added stannous chloride dihydrate (1.34g, 5.95mmol) and then stirred for 3 hr at room temperature. The reaction mixture was washed with dilute sodium hydroxide solution, then water. The organic layer was separated, dried and then evaporated to give 3-amino-N-benzyl-N-methyl-benzamide (270mg, 95%) as solid.
References:
WO2006/123145,2006,A1 Location in patent:Page/Page column 54
121-92-6
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865610-58-8
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865610-58-8
8 suppliers
$118.00/500mg