3-AMINOOXY-N-PROPYL (DIMETHYL-T-BUTYLSILYL) ETHER synthesis

2synthesis methods

Product Name:3-AMINOOXY-N-PROPYL (DIMETHYL-T-BUTYLSILYL) ETHER
CAS Number:114778-46-0
Molecular formula:C9H23NO2Si
Molecular Weight:205.37

73842-99-6 Synthesis

73842-99-6
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3-AMINOOXY-N-PROPYL (DIMETHYL-T-BUTYLSILYL) ETHER

114778-46-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 92 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 16 h / Ambient temperature
2: 84 percent / N-methylhydrazine / CH₂Cl₂ / 1 h / Ambient temperature

References:

Kim, Dae-Kee;Gam, Jongsik;Kim, Young-Woo;Lim, Jinsoo;Kim, Hun-Taek;Kim, Key H. [Journal of Medicinal Chemistry,1997,vol. 40,# 15,p. 2363 - 2373]

1H-Isoindole-1,3(2H)-dione, 2-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propoxy]-

114778-45-9
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114778-46-0
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References