3-Aminopropanoyl chloride synthesis
- Product Name:3-Aminopropanoyl chloride
- CAS Number:5722-81-6
- Molecular formula:C3H6ClNO
- Molecular Weight:107.54
79-37-8
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107-95-9
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5722-81-6
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$116.64/250mgs:
Yield:-
Reaction Conditions:
in N-methyl-acetamide;dichloromethane;
Steps:
6 N-Dansyl 3 Amino Propanoyl Chloride
EXAMPLE 6 N-Dansyl 3 Amino Propanoyl Chloride 970 mg(3 mmol) dansyl beta alanin were dissolved in 5 mL dried dichloromethane and stirred under argon flux at 0° C. Then 0.6 mL (6.6 mmol) oxalyl chloride was added drop wise at 0° C., and subsequently, a few drops of dried dimethylformamide were added which lead to gas development. The mixture was stirred at room temperature for 100 min. The solvents were removed by using a rotary evaporator and then the remainder was twice evaporated with dichloromethane. The crude product was used directly in the next step.
References:
US2009/12279,2009,A1
107-95-9
727 suppliers
$5.00/10g
5722-81-6
5 suppliers
$116.64/250mgs: