(3-bromo-2-fluorophenyl)(methyl)sulfane synthesis
- Product Name:(3-bromo-2-fluorophenyl)(methyl)sulfane
- CAS Number:871353-01-4
- Molecular formula:C7H6BrFS
- Molecular Weight:221.09
1072-85-1
452 suppliers
$5.00/10g
624-92-0
312 suppliers
$26.39/5ml
871353-01-4
22 suppliers
$45.00/10mg
Yield:871353-01-4 70%
Reaction Conditions:
Stage #1: o-fluorobromobenzenewith natrium;N-isopropylpropan-2-amine;isoprene in tetrahydrofuran at -60; for 0.000138889 h;Flow reactor;
Stage #2: (methyldisulfanyl)methane in tetrahydrofuran;Flow reactor;
References:
Weidmann, Niels;Ketels, Marthe;Knochel, Paul [Angewandte Chemie - International Edition,2018,vol. 57,# 33,p. 10748 - 10751][Angew. Chem.,2018,vol. 130,# 33,p. 10908 - 10911,4] Location in patent:supporting information
624-92-0
312 suppliers
$26.39/5ml
871353-01-4
22 suppliers
$45.00/10mg