![](/CAS/GIF/849062-12-0.gif)
3-Bromo-5-methoxybenzeneboronic acid synthesis
- Product Name:3-Bromo-5-methoxybenzeneboronic acid
- CAS Number:849062-12-0
- Molecular formula:C7H8BBrO3
- Molecular Weight:230.85
![Carbon dioxide](/CAS/GIF/124-38-9.gif)
124-38-9
122 suppliers
$175.00/23402
![3,5-Dibromoanisole](/CAS/GIF/74137-36-3.gif)
74137-36-3
210 suppliers
$8.00/1g
![3-Bromo-5-methoxybenzeneboronic acid](/CAS/GIF/849062-12-0.gif)
849062-12-0
70 suppliers
$40.00/50 mg
![3-Borono-5-methoxybenzoic acid](/CAS/GIF/1050424-08-2.gif)
1050424-08-2
26 suppliers
$115.00/50mg
Yield:-
Reaction Conditions:
Stage #1:3,5-dibromoanisole with n-butyllithium in diethyl ether;hexane at -80; for 0.5 h;Inert atmosphere;
Stage #2: with Triisopropyl borate in tetrahydrofuran;diethyl ether;hexane at -70; for 0.5 h;Inert atmosphere;
Stage #3:carbon dioxideFurther stages;
References:
Kurach, Pawel;Lulinski, Sergiusz;Serwatowski, Janusz [European Journal of Organic Chemistry,2008,# 18,p. 3171 - 3178] Location in patent:experimental part