3-Bromophenyl)diphenylphosphine synthesis
- Product Name:3-Bromophenyl)diphenylphosphine
- CAS Number:10212-03-0
- Molecular formula:C18H14BrP
- Molecular Weight:341.18
Yield:10212-03-0 91%
Reaction Conditions:
Stage #1: 1,3-dibromobenzenewith n-butyllithium in tetrahydrofuran;hexane at -90; for 0.75 h;
Stage #2: chloro-diphenylphosphine in tetrahydrofuran;hexane at -90 - 20; for 0.25 h;
References:
Poupon, Jean-Christophe;Boezio, Alessandro A.;Charette, Andre B. [Angewandte Chemie - International Edition,2006,vol. 45,# 9,p. 1415 - 1420]
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