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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

3-Chloro-2-(trimethylsilyl)pyridine synthesis

2synthesis methods
626-60-8 Synthesis
3-Chloropyridine

626-60-8
355 suppliers
$13.00/5g

Chlorotrimethylsilane

75-77-4
564 suppliers
$5.04/10

3-Chloro-2-(trimethylsilyl)pyridine

79698-47-8
24 suppliers
inquiry

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Yield:79698-47-8 80%

Reaction Conditions:

Stage #1: 3-Chloropyridinewith n-butyllithium in hexane at -60; for 1 h;
Stage #2: chloro-trimethyl-silane in tetrahydrofuran at -60 - 20;

References:

Choppin, Sabine;Gros, Philippe;Fort, Yves [European Journal of Organic Chemistry,2001,# 3,p. 603 - 606]

626-60-8 Synthesis
3-Chloropyridine

626-60-8
355 suppliers
$13.00/5g

Chlorotrimethylsilane

75-77-4
564 suppliers
$5.04/10

(3-chloropyridin-4-yl)-trimethylsilane

77332-78-6
2 suppliers
inquiry

3-Chloro-2-(trimethylsilyl)pyridine

79698-47-8
24 suppliers
inquiry

References

3-Chloro-2-(trimethylsilyl)pyridine Related Search:

2-(Trimethylsilyl)pyridine 2-(DIMETHYLSILYL)PYRIDINE