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3-CHLORO-5,6-DIMETHYLPYRIDAZINE-4-CARBONITRILE synthesis

1synthesis methods
40380-36-7 Synthesis
5,6-dimethyl-3-oxo-2H-pyridazine-4-carbonitrile

40380-36-7
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Yield:93824-72-7 90%

Reaction Conditions:

with trichlorophosphate for 3 h;Reflux;

References:

Al-Kamali, Ahmed S. N. [Phosphorus, Sulfur and Silicon and the Related Elements,2009,vol. 184,# 7,p. 1812 - 1824] Location in patent:experimental part