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ChemicalBook CAS DataBase List 3-Chlorophenanthrene

3-Chlorophenanthrene synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: pyridine; hydroxylamine hydrochloride / ethanol / 1 h / 75 °C
2: copper dichloride; tert.-butylnitrite / acetonitrile / 1.33 h / 0 °C

References:

MERCK PATENT GMBH;MUJICA-FERNAUD, TERESA;BUESING, ARNE;VOGES, FRANK;KROEBER, JONAS VALENTIN JP2015/529632, 2015, A