(3-Chloropropyl)sulfaMoyl Chloride synthesis
- Product Name:(3-Chloropropyl)sulfaMoyl Chloride
- CAS Number:42065-72-5
- Molecular formula:C3H7Cl2NO2S
- Molecular Weight:192.06
6276-54-6
372 suppliers
$21.00/25g
42065-72-5
26 suppliers
$200.00/500mg
Yield:42065-72-5 100%
Reaction Conditions:
with sulfuryl dichloride in acetonitrile at 0 - 85;
Steps:
2.a
a) Preparation of 2-a: 1.3 ml (15.4 mmol) sulphuryl chloride were metered into a solution of 1.0 g (7.7 mmol) 3-chloro-propylamine-hydrochloride in 10 ml acetonitrile while cooling with an ice bath and stirred overnight at 85° C. Then the reaction solution was evaporated down i. vac. This gave a quantitative yield of 2-a.
References:
US2009/42867,2009,A1 Location in patent:Page/Page column 40
7791-25-5
254 suppliers
$15.00/0.5g
6276-54-6
372 suppliers
$21.00/25g
42065-72-5
26 suppliers
$200.00/500mg