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66416-52-2

3-Cyano-2-methyl-6-phenylpyridine synthesis

3synthesis methods
1118-61-2 Synthesis
3-Aminocrotononitrile

1118-61-2
250 suppliers
$9.00/25g

4187-87-5 Synthesis
1-PHENYL-2-PROPYN-1-OL

4187-87-5
168 suppliers
$9.00/1g

3-Cyano-2-methyl-6-phenylpyridine

66416-52-2
7 suppliers
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Yield:66416-52-2 86%

Reaction Conditions:

with barium manganate in ethanol;acetic acid at 170; for 0.75 h;Microwave irradiation;Bohlmann-Rahtz reaction;

References:

Bagley, Mark C.;Lin, Zhifan;Pope, Simon J. A. [Chemical Communications,2009,# 34,p. 5165 - 5167] Location in patent:supporting information; experimental part