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73013-50-0

(3-CYANOPHENYL)ACETONE synthesis

8synthesis methods
-

Yield:73013-50-0 77%

Reaction Conditions:

Stage #1: m-cyanoanilinewith methanesulfonic acid;2,2-dimethylpropyl nitrite in water;acetone at 25; for 0.166667 h;Green chemistry;
Stage #2: Isopropenyl acetate in water;acetone at 20; for 6 h;Irradiation;Green chemistry;

References:

Wang, Liang;Shen, Jun;Yang, Sen;Liu, Wenjie;Chen, Qun;He, Mingyang [Green Chemistry,2018,vol. 20,# 6,p. 1290 - 1296] Location in patent:supporting information