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ChemicalBook CAS DataBase List 3-Cyclohexen-1-ol, 4-bromo-, 1-benzoate

3-Cyclohexen-1-ol, 4-bromo-, 1-benzoate synthesis

5synthesis methods
-

Yield:1450812-66-4 91%

Reaction Conditions:

with triphenyl phosphite;bromine;triethylamine in dichloromethane at -60 - 20; for 20 h;Inert atmosphere;Reflux;

References:

Zhan, Fuxu;Liang, Guangxin [Angewandte Chemie - International Edition,2013,vol. 52,# 4,p. 1266 - 1269][Angew. Chem.,2012,vol. 125,# 4,p. 1304 - 1307,4] Location in patent:supporting information