3-(CYCLOHEXYLOXY)PROPAN-1-AMINE synthesis

3synthesis methods

Product Name:3-(CYCLOHEXYLOXY)PROPAN-1-AMINE
CAS Number:16728-63-5
Molecular formula:C9H19NO
Molecular Weight:157.25

3-(cyclohexyloxy)propanoic acid(WXC08556)

27912-81-8
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16728-63-5
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: LAH / diethyl ether / 0 °C
2: Et₃N / dimethylformamide / 1 h / 0 °C
3: NaN₃ / dimethylformamide; H₂O / 60 - 70 °C
4: H₂O, Ph₃P / tetrahydrofuran / Ambient temperature

References:

Takeuchi, Kumiko;Kohn, Todd J.;True, Timothy A.;Mais, Dale E.;Wikel, James H.;Utterback, Barbara G.;Wyss, Virginia L.;Jakubowski, Joseph A. [Journal of Medicinal Chemistry,1998,vol. 41,# 27,p. 5362 - 5374]

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References

1-Propanol, 3-(cyclohexyloxy)-, methanesulfonate

823226-18-2
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16728-63-5
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References

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