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ChemicalBook CAS DataBase List 3-DEOXY-3-FLUORO-D-GLUCOSE

3-DEOXY-3-FLUORO-D-GLUCOSE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 1.5 h / -20 °C
2: cesium fluoride / tert-butyl alcohol / 26 h / 80 °C
3: Dowex 50W X8, H+ / water; 1,4-dioxane / 18 h / 65 °C

References:

Liu, Zilei;Jenkinson, Sarah F.;Vermaas, Tom;Adachi, Isao;Wormald, Mark R.;Hata, Yukako;Kurashima, Yukiko;Kaji, Akira;Yu, Chu-Yi;Kato, Atsushi;Fleet, George W. J. [Journal of Organic Chemistry,2015,vol. 80,# 9,p. 4244 - 4258]

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