3-[dimethyl(phenyl)silyl]propan-1-ol synthesis

12synthesis methods

Product Name:3-[dimethyl(phenyl)silyl]propan-1-ol
CAS Number:68469-62-5
Molecular formula:C11H18OSi
Molecular Weight:194.35

2632-95-3
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68469-62-5
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Yield:68469-62-5 71%

Reaction Conditions:

Stage #1: γ-chloropropyldimethylphenylsilanewith magnesium in tetrahydrofuran;Metallation;
Stage #2: with oxygen in tetrahydrofuran; for 2 h;Oxidation;

References:

Fujiyama;Nakashima;Kim;Fujio;Tsuno [Bulletin of the Chemical Society of Japan,2000,vol. 73,# 2,p. 429 - 438]

768-33-2
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68469-62-5
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3292-88-4
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591-51-5
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766-77-8
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$12.00/5g

68469-62-5
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10605-40-0
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$50.00/1g

68469-62-5
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