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153813-81-1

3-(diMethylaMino)-1-(3-nitrophenyl)prop-2-en-1-one synthesis

1synthesis methods
577-59-3 Synthesis
2-Nitroacetophenone

577-59-3
274 suppliers
$6.00/5g

4637-24-5 Synthesis
N,N-Dimethylformamide dimethyl acetal

4637-24-5
604 suppliers
$5.00/25g

3-(diMethylaMino)-1-(3-nitrophenyl)prop-2-en-1-one

153813-81-1
19 suppliers
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Yield:153813-81-1 95%

Reaction Conditions:

in N,N-dimethyl-formamide at 100; for 0.75 h;Inert atmosphere;

References:

Bunce, Richard A.;Nammalwar, Baskar [Organic Preparations and Procedures International,2010,vol. 42,# 6,p. 557 - 563] Location in patent:experimental part