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ChemicalBook CAS DataBase List 3-Ethoxy-1-chloro-2-propanol

3-Ethoxy-1-chloro-2-propanol synthesis

7synthesis methods
-

Yield:-

Reaction Conditions:

with molybdenum incorporated SBA-15 mesoporous silica at 122.84; for 0.5 h;Catalytic behavior;

Steps:

2.3 Catalytic studies
General procedure: In a typical experiment, a 20 mL sample vial was charged with a certain amount of desired catalyst followed by 1.1 mmol of epoxide and 3 mL of alcohol. The reaction was stirred using magnetic stir bar at ambient temperature (396 K ± 2 K). The reaction mixture was withdrawn at regular intervals and injected into a gas chromatograph (HP 5890, FID detector and DB-5 capillary column) to monitor the progress of the reaction. Reactant conversion was calculated with respect to epoxide since alcohols were used in excess as the solvent and nucleophile.

References:

Budhi, Sridhar;Peeraphatdit, Chorthip;Pylypenko, Svitlana;Nguyen, Vy H.T.;Smith, Emily A.;Trewyn, Brian G. [Applied Catalysis A: General,2014,vol. 475,p. 469 - 476]

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