3-ETHOXYACRYLIC ACID synthesis
- Product Name:3-ETHOXYACRYLIC ACID
- CAS Number:6192-01-4
- Molecular formula:C5H8O3
- Molecular Weight:116.12
122-51-0
487 suppliers
$10.00/5ml
6192-01-4
124 suppliers
$12.00/1g
Yield:6192-01-4 79%
Reaction Conditions:
with acetic anhydride
Steps:
Synthesis of ethyl 2-(2,3,4,5-tertrafluorobenzoyl)-3-ethoxyacrylate, Compound j.
Synthesis of ethyl 2-(2,3,4,5-tertrafluorobenzoyl)-3-ethoxyacrylate, Compound j. A mixture of compound i (22 g, 83 mmol), triethyl orthoformate (17 g, 115 mmol), and 20 g of acetic anhydride was heated at 150° C. with stirring for 2 hours. Removal of the solvent in vacuo gave the crude product for next step, yield 79%.
References:
Zhi, Chengxin;Wright, George E. US2003/181719, 2003, A1
1001-26-9
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$6.00/1g
6192-01-4
124 suppliers
$12.00/1g
61310-53-0
136 suppliers
$41.00/25mL
6192-01-4
124 suppliers
$12.00/1g
6191-99-7
162 suppliers
$24.00/1g
6192-01-4
124 suppliers
$12.00/1g
10601-80-6
304 suppliers
$6.00/5g
6192-01-4
124 suppliers
$12.00/1g