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ChemicalBook CAS DataBase List 3'-FLUORO-4'-METHYLPROPIOPHENONE

3'-FLUORO-4'-METHYLPROPIOPHENONE synthesis

2synthesis methods
-

Yield:107076-07-3 59%

Reaction Conditions:

with (1,2-dimethoxyethane)dichloronickel(II);5, 6-dimethyl-1,10-phenanthroline;[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate;N-ethyl-N,N-diisopropylamine;triphenylphosphine in acetonitrile at 20; under 760.051 Torr; for 2 h;Irradiation;Inert atmosphere;Sealed tube;Schlenk technique;

References:

Zhang, Lili;Chen, Shuai;He, Hengchi;Li, Weipeng;Zhu, Chengjian;Xie, Jin [Chemical Communications,2021,vol. 57,# 72,p. 9064 - 9067] Location in patent:supporting information