3'-HYDROXY-2,4,4TRIBROMODIPHENYL ETHER synthesis

2synthesis methods

Product Name:3'-HYDROXY-2,4,4TRIBROMODIPHENYL ETHER
CAS Number:24949-30-2
Molecular formula:C12H7Br3O2
Molecular Weight:422.89

602326-17-0
0 suppliers
inquiry

24949-30-2
3 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: KH₂PO₄; CF₃CO₃H / CH₂Cl₂ / 2 h / 0 °C
1.2: 83 percent / hydrochloric acid / methanol / 15 h
2.1: 29 percent / bromine; tert-butylamine / CH₂Cl₂; toluene / 6 h / -70 - -60 °C

References:

Marsh, Goeran;Stenutz, Roland;Bergman, Ake [European Journal of Organic Chemistry,2003,# 14,p. 2566 - 2576]

602326-18-1
0 suppliers
inquiry

24949-30-2
3 suppliers
inquiry

Phenol, 2,6-dibromo-3-(2,4-dibromophenoxy)-

24949-31-3
0 suppliers
inquiry

References

3'-HYDROXY-2,4,4TRIBROMODIPHENYL ETHER Related Search:

2,4,4'-TRIBROMODIPHENYL ETHER