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3-HYDROXY-2-METHOXYBENZOIC ACID synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C
3: lithium hydroxide monohydrate; lithium hydroxide monohydrate / tetrahydrofuran / 4 h / 20 °C

References:

WO2022/126000,2022,A1

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