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ChemicalBook CAS DataBase List 3-HYDROXY-5-METHYLMERCAPTO-1,2,4-THIADIAZOLE

3-HYDROXY-5-METHYLMERCAPTO-1,2,4-THIADIAZOLE synthesis

3synthesis methods
-

Yield:56409-41-7 40%

Reaction Conditions:

Stage #1: potassium cyanocarbonimidodithioate;dimethyl sulfate in water at 20; for 2 h;
Stage #2: with hydrogenchloride;dihydrogen peroxide in water; pH=2 - 3; for 0.5 h;

References:

WO2005/7636,2005,A1 Location in patent:Page/Page column 19