3-Hydroxy-6-methylbenzo[d][1,2,3]triazin-4(3H)-one synthesis
- Product Name:3-Hydroxy-6-methylbenzo[d][1,2,3]triazin-4(3H)-one
- CAS Number:132533-58-5
- Molecular formula:C8H7N3O2
- Molecular Weight:177.16
2941-78-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sulfuric acid / 48 h / Reflux
2: hydroxylamine hydrochloride; ammonium hydroxide / methanol / 48 h
3: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C
References:
Shi, Wei-Min;Ma, Xiao-Pan;Pan, Cheng-Xue;Su, Gui-Fa;Mo, Dong-Liang [Journal of Organic Chemistry,2015,vol. 80,# 21,p. 11175 - 11183]
18595-16-9
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