![](/CAS/GIF/4368-06-3.gif)
3-HYDROXYBUTYRONITRILE synthesis
- Product Name:3-HYDROXYBUTYRONITRILE
- CAS Number:4368-06-3
- Molecular formula:C4H7NO
- Molecular Weight:85.1
![Acetoacetamide](/CAS/GIF/5977-14-0.gif)
5977-14-0
171 suppliers
$35.70/100g
![3-HYDROXYBUTYRONITRILE](/CAS/GIF/4368-06-3.gif)
4368-06-3
24 suppliers
$150.00/1g
Yield: 85 %Chromat.
Reaction Conditions:
with Triethoxysilane;[cis-Fe(H)(SPh)(PMe3)4] in tetrahydrofuran at 60; for 24 h;Inert atmosphere;
Steps:
2.2. General procedure for the dehydration of amides to nitriles
General procedure: To a 25ml Schlenk tube containing a solution of 1 in 2ml of THF was added amide (1.0 mmol) and (EtO)3SiH (0.50 g, 3.0 mmol). The reaction mixture was stirred at 60 °C until there was no amide left (monitored by TLC and GC-MS). The product was purified according to literature procedures by Beller [27].
References:
Xue, Benjing;Sun, Hongjian;Wang, Yan;Zheng, Tingting;Li, Xiaoyan;Fuhr, Olaf;Fenske, Dieter [Catalysis Communications,2016,vol. 86,p. 148 - 150]
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141-78-6
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$20.50/250ml
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75-05-8
967 suppliers
$10.00/10g
![3-HYDROXYBUTYRONITRILE](/CAS/GIF/4368-06-3.gif)
4368-06-3
24 suppliers
$150.00/1g
![1-Chloro-2-propanol](/CAS/GIF/127-00-4.gif)
127-00-4
132 suppliers
$25.19/25g
![3-HYDROXYBUTYRONITRILE](/CAS/GIF/4368-06-3.gif)
4368-06-3
24 suppliers
$150.00/1g
![Crotononitrile (pract)](/CAS/GIF/4786-20-3.gif)
4786-20-3
66 suppliers
$9.00/1g
![3-HYDROXYBUTYRONITRILE](/CAS/GIF/4368-06-3.gif)
4368-06-3
24 suppliers
$150.00/1g