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3-Iodcatechol synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 - 5 °C
1.2: 2 h / -78 - 20 °C
2.1: boron tribromide / dichloromethane / 3 h / 0 - 20 °C

References:

LG Chem, Ltd.;KIM, Young Kwan;PARK, Sang Yun;JOO, Hyun Woo;CHOI, Eun Sil;PAEK, Seung Yup;KANG, Seung Wan;KIM, Byung Gyu;LEE, Chang Seok;KIM, Sung Wook;LEE, Sang Dae EP3239143, 2017, A2