ChemicalBook CAS DataBase List 3-Methoxy-2-Nitro Benzonitrile

3-Methoxy-2-Nitro Benzonitrile synthesis

3synthesis methods

Product Name:3-Methoxy-2-Nitro Benzonitrile
CAS Number:142596-50-7
Molecular formula:C8H6N2O3
Molecular Weight:178.14

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: SOCl₂ / CH₂Cl₂ / 2 h / Heating
2: aq. NH₃ / tetrahydrofuran / 0.5 h / Ambient temperature
3: 74.5 percent / SOCl₂ / tetrahydrofuran / Ambient temperature

References:

Goto;Nakamura;Morioka;Kondo;Naito;Tsutsumi [Chemical and Pharmaceutical Bulletin,1996,vol. 44,# 3,p. 547 - 551]

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99595-85-4
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142596-50-7
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References

15865-57-3
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142596-50-7
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References

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