3-Methoxy-4-(trifluoroMethyl)benzyl alcohol, 97% synthesis
- Product Name:3-Methoxy-4-(trifluoroMethyl)benzyl alcohol, 97%
- CAS Number:276861-64-4
- Molecular formula:C9H9F3O2
- Molecular Weight:206.16
276861-63-3
60 suppliers
$18.00/250mg
276861-64-4
26 suppliers
$51.10/1g
Yield:276861-64-4 90 %
Reaction Conditions:
Stage #1: 3-methoxy-4-(trifluoromethyl)benzoic acidwith sodium tetrahydroborate in tetrahydrofuran at 0;Inert atmosphere;
Stage #2: with boron trifluoride diethyl etherate in tetrahydrofuran at 20;Inert atmosphere;
References:
Deguchi, Hiroki;Hanaya, Kengo;Sugai, Takeshi;Higashibayashi, Shuhei [Chemical Communications,2022,vol. 59,# 6,p. 748 - 751] Location in patent:supporting information