Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

((3-METHOXYPHENYL)ETHYNYL)-TRIMETHYLSIL& synthesis

4synthesis methods
-

Yield:40230-92-0 98%

Steps:

28.a a

a (3-Methoxy-phenylethynyl)-trimethyl-silane The title compound was synthesised from commercially available 1-iodo-3-methoxy-benzene using the procedure described in Example 18, step (a), in 98% yield. 1H NMR (CDCl3) δ7.23 (t, 1H, J=7.8 Hz), 7.08 (dt, 1H, J=1.2, 7.6 Hz), 7.02 (m, 1H), 6.89 (m, 1H), 3.82 (s, 3H), 0.28 (s, 9H).

References:

US2002/169200,2002,A1