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ChemicalBook CAS DataBase List 3-METHOXYTHIETANE

3-METHOXYTHIETANE synthesis

2synthesis methods
201230-82-2 Synthesis
carbon monoxide

201230-82-2
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3-METHOXYTHIETANE

117471-38-2
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2(3H)-Thiophenone, dihydro-3-methoxy-

96862-65-6
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Yield:96862-65-6 87%

Reaction Conditions:

dicobalt octacarbonyl;triruthenium dodecacarbonyl in 1,2-dimethoxyethane at 145; under 45600 Torr; for 48 h;

References:

Wang, Ming-De;Calet, Serge;Alper, Howard [Journal of Organic Chemistry,1989,vol. 54,# 1,p. 20 - 21]