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13834-53-2

3-Methyl-1H-Thieno[3,2-c]pyrazole synthesis

1synthesis methods
1-Thiophen-2-yl-ethanone (4-nitro-phenyl)-hydrazone

349476-10-4
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3-Methyl-1H-Thieno[3,2-c]pyrazole

13834-53-2
2 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: polyphosphoric acid / 160 °C
2: SnCl2, aq. HCl / acetic acid
3: aq. Na2Cr2O7, aq. H2SO4 / 0 °C

References:

Dennler,E.B.;Frasca,A.R. [Canadian Journal of Chemistry,1967,vol. 45,p. 697 - 705]