3-METHYL-4-PHENYL-1-BUTENE synthesis
- Product Name:3-METHYL-4-PHENYL-1-BUTENE
- CAS Number:6683-51-8
- Molecular formula:C11H14
- Molecular Weight:146.23
2344-70-9
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Yield:6683-51-8 95 %Chromat.
Reaction Conditions:
with potassium tert-butylate;C29H30ClNOP2Ru(1+) in acetone at 60; for 1 h;Product distribution / selectivity;Inert atmosphere;
Steps:
14
The ruthenium complex 2 which has been produced in the Example 1 and OlBu were added to a Schlenk flask in which boiling chips are added. Subsequently, the substrate described the Table 4 below and acetone were added thereto. The mixture was then stirred at 60 degrees C under nitrogen stream. As a result, the ketones that correspond to the reacting compound (i.e., substrate) described in the Table 4 were obtained. The results are given in the following Table 4.
References:
WO2012/144650,2012,A1 Location in patent:Page/Page column 46-48
