3-(Methylsulfonylamino)benzylamine Hydrochloride synthesis
- Product Name:3-(Methylsulfonylamino)benzylamine Hydrochloride
- CAS Number:238428-26-7
- Molecular formula:C8H12N2O2S.ClH
- Molecular Weight:236.722
238427-66-2
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Yield:238428-26-7 100%
Reaction Conditions:
with hydrogenchloride in 1,4-dioxane at 20; for 1 h;
Steps:
B; 2010.B
To the intermediate from Step A above (407 mg) was added hydrogen chloride (4M in dioxane, 5 mL) and the suspension was stirred at room temperature for 1 h. The reaction mixture was evaporated to afford the title compound as a colourless solid (350 mg; quantitative). [M-NH3Cl]+=184.
References:
US2006/173183,2006,A1 Location in patent:Page/Page column 84
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238428-26-7
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$37.00/100mg
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