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ChemicalBook CAS DataBase List 3-(N-HYDROXYAMINO)PROPYL PHOSPHONATE
66508-11-0

3-(N-HYDROXYAMINO)PROPYL PHOSPHONATE synthesis

6synthesis methods
Phosphonic acid, P-[3-[(phenylmethoxy)amino]propyl]-, diethyl ester

557090-55-8
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Yield:66508-11-0 82%

Reaction Conditions:

Stage #1: O-(benzylhydroxylamino)propylphosphonic acid diethyl esterwith hydrogenchloride;acetic acid in water; for 14 h;Heating;
Stage #2: with pyridine in ethanol; pH=5;

References:

B?azewska, Katarzyna;Gajda, Tadeusz [Tetrahedron,2003,vol. 59,# 51,p. 10249 - 10254]