3-(n-Pentyloxy)benzoic acid synthesis
- Product Name:3-(n-Pentyloxy)benzoic acid
- CAS Number:110698-30-1
- Molecular formula:C12H16O3
- Molecular Weight:208.25
132858-17-4
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Yield:-
Reaction Conditions:
with lithium hydroxide in tetrahydrofuran;methanol;water at 20;
Steps:
General synthetic procedure for intermediates 13a-o.
General procedure: Step 2: The respective ester was dissolved in THF: CH3OH: H2O (3:3:1), and aqueous LiOH solution (1.0 equiv) was added slowly. The mixture was then stirred at room temperature for 2 h. The solvent was evaporated in vacuum, the product was precipitated by addition of 2 M HCl until a pH of ≤ 2 was reached, filtered off, and dried in vacuum to get intermediates 13a-o.
References:
Hu, Lijun;Ren, Qiang;Deng, Liming;Zhou, Zongtao;Cai, Zongyu;Wang, Bin;Li, Zheng [European Journal of Medicinal Chemistry,2021,vol. 211] Location in patent:supporting information
24083-06-5
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$150.00/500mg
110698-30-1
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110-53-2
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7781-98-8
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19438-10-9
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$6.00/5g
110698-30-1
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