3-(β-nitro-β-methylvinyl)indole synthesis
- Product Name:3-(β-nitro-β-methylvinyl)indole
- CAS Number:64252-02-4
- Molecular formula:C11H10N2O2
- Molecular Weight:202.21
83-34-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) 2,3-dichloro-5,6-dicyan-p-benzoquinone; 2.) potassium carbonate / 1.) tetrahydrofuran, water, room temperature, 10 h; 2.) 1 h
2: 75 percent / ammonium acetate / 2 h / 120 - 130 °C
References:
Canoira;Gonzalo Rodriguez;Subirats;Escario;Jimenez;Martinez-Fernandez [European Journal of Medicinal Chemistry,1989,vol. 24,# 1,p. 39 - 42]
