![](/CAS/GIF/5023-94-9.gif)
3-NITROBENZAMIDOXIME synthesis
- Product Name:3-NITROBENZAMIDOXIME
- CAS Number:5023-94-9
- Molecular formula:C7H7N3O3
- Molecular Weight:181.15
![3-Nitrobenzonitrile](/CAS/GIF/619-24-9.gif)
619-24-9
262 suppliers
$10.00/1g
![3-NITROBENZAMIDOXIME](/CAS/GIF/5023-94-9.gif)
5023-94-9
42 suppliers
$35.00/1g
Yield:5023-94-9 100%
Reaction Conditions:
with hydroxylamine in ethanol;water at 80; for 5 h;
Steps:
4.1.2. General Procedure for the Automated Synthesis of Compounds 6 and 7
General procedure: Nitrile (20.00 mmol), ethanol (30.0 mL) and hydroxylamine (50% in water, 2.0 mL) were addedin a 75 mL double jacket reactor from Chemspeed equipped with condenser. The mixture was shakenat 600 rpm for 5 h at 80 °C, then cooled down to 20 °C. The reaction medium was evaporated underreduced pressure and the solid was finally dried overnight in a heated (40 °C) vacuum oven. 3,4-(Methylenedioxy)benzamidoxime (6): White solid, yield: quant. 1H-NMR (300MHz, DMSO) δ ppm:9.51 (s, 1H), 7.22-7.16 (m, 2H), 6.93-6.88 (m, 1H), 6.03 (s, 2H), 5.72 (s, 2H). 13C-NMR (125.75 MHz,DMSO) δ ppm: 150.98, 148.25, 147.56, 127.87, 119.75, 108.30, 106.17, 101.61.
References:
Stevanovic, Strahinja;Sencanski, Milan;Danel, Mathieu;Menendez, Christophe;Belguedj, Roumaissa;Bouraiou, Abdelmalek;Nikolic, Katarina;Cojean, Sandrine;Loiseau, Philippe M.;Glisic, Sanja;Baltas, Michel;García-Sosa, Alfonso T. [Molecules,2019,vol. 24,# 7,art. no. 1282]
![2λ4-1,2,3,5-Oxathiadiazol-2-amine, 4-(3-nitrophenyl)- (9CI)](/CAS/20210305/GIF/172469-58-8.gif)
172469-58-8
0 suppliers
inquiry
![3-NITROBENZAMIDOXIME](/CAS/GIF/5023-94-9.gif)
5023-94-9
42 suppliers
$35.00/1g
![ALPHA-CHLORO-3-NITROBENZALDOXIME](/CAS/GIF/33512-94-6.gif)
33512-94-6
29 suppliers
$45.00/10mg
![3-NITROBENZAMIDOXIME](/CAS/GIF/5023-94-9.gif)
5023-94-9
42 suppliers
$35.00/1g
![3-Bromonitrobenzene](/CAS/GIF/585-79-5.gif)
585-79-5
7 suppliers
$15.00/1g
![3-NITROBENZAMIDOXIME](/CAS/GIF/5023-94-9.gif)
5023-94-9
42 suppliers
$35.00/1g