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(3-NITROBENZYL)MERCAPTAN 97 synthesis

4synthesis methods
1335107-28-2 Synthesis
O-ethyl S-3-nitrobenzyl carbonodithioate

1335107-28-2
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Yield:77472-39-0 88%

Reaction Conditions:

with hydrogenchloride;ethylenediamine in water;dimethyl sulfoxide; for 0.0833333 h;

References:

Morgan, M. Thomas;Bagchi, Pritha;Fahrni, Christoph J. [Journal of the American Chemical Society,2011,vol. 133,# 40,p. 15906 - 15909] Location in patent:supporting information; experimental part