![](/CAS/GIF/2613-26-5.gif)
3-NITROPHENYLSULFUR PENTAFLUORIDE synthesis
- Product Name:3-NITROPHENYLSULFUR PENTAFLUORIDE
- CAS Number:2613-26-5
- Molecular formula:C6H4F5NO2S
- Molecular Weight:249.16
![Phenyl sulfur pentafluoride](/CAS/GIF/2557-81-5.gif)
2557-81-5
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2613-26-5
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Yield: 100%
Reaction Conditions:
with nitronium tetrafluoborate;trifluorormethanesulfonic acid in dichloromethane at 20; for 24 h;Reagent/catalyst;Solvent;Temperature;Time;
Steps:
5
PhSF5 15 reacts with NO2+BF4/TfOH in CH2Cl2 at room temperature to give 1-nitro-3-(pentafluorosulfanyl)benzene 16 in near quantitative yield, as seen in Table 6.
References:
University of North Florida;Laali, Kenneth K. US9238660, 2016, B1 Location in patent:Page/Page column 10; 11
![Bis(3-nitrophenyl) disulfide](/CAS/GIF/537-91-7.gif)
537-91-7
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2613-26-5
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![Phenyl sulfur pentafluoride](/CAS/GIF/2557-81-5.gif)
2557-81-5
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$25.00/250mg
![1-Pentafluorosulfanyl-3,5-dinitrobenzene](/CAS/GIF/142653-59-6.gif)
142653-59-6
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![3-NITROBENZENESULPHONYL FLUORIDE 97](/CAS/GIF/349-78-0.gif)
349-78-0
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$29.00/1g
![3-NITROPHENYLSULFUR PENTAFLUORIDE](/CAS/GIF/2613-26-5.gif)
2613-26-5
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![1,4-Cyclohexadiene, (1E,4Z)-](/CAS/20200331/GIF/1165952-92-0.gif)
1165952-92-0
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2613-26-5
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89415-83-8
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![3-NITROPHENYLSULFUR PENTAFLUORIDE](/CAS/GIF/2613-26-5.gif)
2613-26-5
79 suppliers
$15.00/1g