3-(o-Tolyloxy)pyridine synthesis
3synthesis methods
- Product Name:3-(o-Tolyloxy)pyridine
- CAS Number:33399-54-1
- Molecular formula:C12H11NO
- Molecular Weight:185.22
Yield:33399-54-1 96%
Reaction Conditions:
with 2-acetonylpyridine;caesium carbonate;copper(I) bromide in dimethyl sulfoxide at 80; for 9 h;Inert atmosphere;chemoselective reaction;
References:
Zhang, Qi;Wang, Deping;Wang, Xianyang;Ding, Ke [Journal of Organic Chemistry,2009,vol. 74,# 18,p. 7187 - 7190] Location in patent:supporting information; experimental part
