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3-Penten-2-one, 4-(methylamino)-, (E)- (9CI) synthesis

1synthesis methods
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Yield:88636-30-0 92% ,130256-90-5 92%

Reaction Conditions:

in pentane;Ar atmosphere, stirring (1 h, 25°C); pptn. of MeC(O)CHCMeNHMe on cooling (-78°C), B-compound from filtrate by evapn. (14 Torr);

References:

Koester, Roland;Seidel, Guenter;Boese, Roland;Wrackmeyer, Bernd [Chemische Berichte,1988,vol. 121,p. 597 - 616]

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