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ChemicalBook CAS DataBase List 3-PHENYL-2-(PHENYLSULFONYL)-1,2-OXAZIRIDINE

3-PHENYL-2-(PHENYLSULFONYL)-1,2-OXAZIRIDINE synthesis

2synthesis methods
3-Phenyl-2-(phenylsulfonyl)-1,2-oxaziridine is a heterocyclic hydrocarbon derivative, mainly used as an organic pharmaceutical intermediate. 
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: triethylamine / diethyl ether; dichloromethane / 1.08 h / -78 - 0 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C
2.2: 3 h / -78 - 20 °C
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 - -40 °C
3.2: 2 h / -78 °C

References:

SPEEDEL EXPERIMENTA AG WO2007/141318, 2007, A1