3-PHENYLPYRAZINAMINE synthesis

8synthesis methods

Product Name:3-PHENYLPYRAZINAMINE
CAS Number:41270-67-1
Molecular formula:C10H9N3
Molecular Weight:171.2

7677-24-9 Synthesis

7677-24-9
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$19.00/5g

100-52-7 Synthesis

100-52-7
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$20.37/250g

107-15-3
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$11.19/25ML

41270-67-1
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Yield:41270-67-1 120 mg

Reaction Conditions:

Stage #1: benzaldehyde;ethylenediamine in 1,4-dioxane at 70; for 0.25 h;
Stage #2: trimethylsilyl cyanidewith oxygen;1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane at 25 - 27; for 3 h;
Stage #3: with manganese(IV) oxide;potassium hydroxide in 1,4-dioxane;methanol at 25 - 27;

References:

Guchhait, Sankar K.;Priyadarshani, Garima;Gulghane, Nikhil M. [RSC Advances,2016,vol. 6,# 61,p. 56056 - 56063]