![](/CAS/GIF/76196-67-3.gif)
3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI) synthesis
- Product Name:3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI)
- CAS Number:76196-67-3
- Molecular formula:C7H8N2O2
- Molecular Weight:152.15
![6-CYANONICOTINIC ACID](/CAS/GIF/70165-31-0.gif)
70165-31-0
138 suppliers
$28.00/250mg
![3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI)](/CAS/GIF/76196-67-3.gif)
76196-67-3
25 suppliers
$45.00/2.5mg
Yield:76196-67-3 750 mg
Reaction Conditions:
with 10% palladium hydroxide on charcoal;hydrogen in methanol at 20;
Steps:
24.1 Step 1: Preparation of 6-(aminomethyl)nicotinic acid
To a solution of 6-Cyanonicotinic acid (1 g, 6.7 mmol) in MeOH (20 mL) was added Pd(OH)2(10% Pd in carbon, 0.1 g). The mixture was stirred at r.t. under a hydrogen atmosphere overnight. Then the mixture was diluted with H20 (10 mL), the catalyst was filtered, and the filtrate was concentrated in vacuo to give 6-(aminomethyl)nicotinic acid (750 mg), which was used in the next step without further purification.
References:
WO2019/118612,2019,A1 Location in patent:Paragraph 0205
![6-Aminomethyl-nicotinic acid methyl ester](/CAS/GIF/139183-87-2.gif)
139183-87-2
46 suppliers
$110.00/50mg
![3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI)](/CAS/GIF/76196-67-3.gif)
76196-67-3
25 suppliers
$45.00/2.5mg
![6-Methylnicotinic acid](/CAS/GIF/3222-47-7.gif)
3222-47-7
337 suppliers
$6.00/1g
![3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI)](/CAS/GIF/76196-67-3.gif)
76196-67-3
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$45.00/2.5mg
![Methyl 6-methylnicotinate](/CAS/GIF/5470-70-2.gif)
5470-70-2
511 suppliers
$5.00/5g
![3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI)](/CAS/GIF/76196-67-3.gif)
76196-67-3
25 suppliers
$45.00/2.5mg
![methyl 6-(bromomethyl)nicotinate](/CAS/GIF/131803-48-0.gif)
131803-48-0
108 suppliers
$51.00/100mg
![3-Pyridinecarboxylicacid,6-(aminomethyl)-(9CI)](/CAS/GIF/76196-67-3.gif)
76196-67-3
25 suppliers
$45.00/2.5mg