3-PyrrolidinaMine, N,1-diethyl- synthesis
- Product Name:3-PyrrolidinaMine, N,1-diethyl-
- CAS Number:108963-17-3
- Molecular formula:C8H18N2
- Molecular Weight:142.24
325775-36-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 20 °C
2.2: 50 °C
3.1: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / 760.05 Torr
References:
Zhou, Jie;Ji, Ming;Yao, Haiping;Cao, Ran;Zhao, Hailong;Wang, Xiaoyu;Chen, Xiaoguang;Xu, Bailing [Organic and Biomolecular Chemistry,2018,vol. 16,# 17,p. 3189 - 3202]
186550-13-0
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108963-17-3
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