ChemicalBook CAS DataBase List 3-Quinolinepropanoicacid,-alpha--amino-,(S)-(9CI)

3-Quinolinepropanoicacid,-alpha--amino-,(S)-(9CI) synthesis

2synthesis methods

Product Name:3-Quinolinepropanoicacid,-alpha--amino-,(S)-(9CI)
CAS Number:135213-90-0
Molecular formula:C12H12N2O2
Molecular Weight:216.24

104325-51-1
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3-Quinolinepropanoicacid,-alpha--amino-,(S)-(9CI)

135213-90-0
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF a) 90 deg C, 6 h, b) RT, overnight
2: 6 M aq. NaOH / aq. ethanol / 1.5 h / Ambient temperature
3: dioxane / 3 h / Heating
5: 6 M aq. HCl / 4 h / Heating

References:

Acosta, C. Kirk;Bahr, Martin L.;Burdett, James E.;Cessac, James W.;Martinez, Rudy A.;et al. [Journal of Chemical Research, Miniprint,1991,# 5,p. 914 - 934]

Propanedioic acid, 2-(acetylamino)-2-(3-quinolinylmethyl)-, 1,3-diethyl ester

120652-19-9
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135213-90-0
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References