3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID synthesis
- Product Name:3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID
- CAS Number:676348-90-6
- Molecular formula:C12H23NO4
- Molecular Weight:245.32
24424-99-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: diethyl ether / 6 h / 20 °C
2.1: O3 / CH2Cl2; methanol / 2 h / -78 °C
2.2: Me2S / CH2Cl2; methanol / 1 h / -78 - 20 °C
3.1: aq. NaClO2; NaH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol / 1 h / 20 °C
References:
Ramachandran, P. Veeraraghavan;Burghardt, Thomas E. [Chemistry - A European Journal,2005,vol. 11,# 15,p. 4387 - 4395]
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