3-tert-Butyl-9H-carbazole synthesis
- Product Name:3-tert-Butyl-9H-carbazole
- CAS Number:22401-74-7
- Molecular formula:C16H17N
- Molecular Weight:223.31
22401-71-4
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22401-74-7
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Yield: 95%
Reaction Conditions:
palladium 10% on activated carbon in 1,3,5-trimethyl-benzene at 180 - 190; for 30 h;Heating / reflux;
Steps:
1.2
A 2L flask equipped with an over head stirrer, nitrogen bubbler and reflux condenser was charged with tetrahydrobutylcarbonate (79g, 0.34mol), 10 % Pd/C (11.1g, 0.004mol) and trimethylbenzene. The reaction mixture was heated to reflux (180-1900C) for 30h and then allowed to cool to room temperature. Upon cooling the reaction mixture EPO
References:
CAMBRIDGE DISPLAY TECHNOLOGY LIMITED;CDT OXFORD LIMITED WO2006/70185, 2006, A1 Location in patent:Page/Page column 28; 29
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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22401-74-7
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$74.00/200mg
507-20-0
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86-74-8
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22401-74-7
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$74.00/200mg
4496-49-5
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22401-74-7
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$74.00/200mg
98-53-3
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100-63-0
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22401-74-7
44 suppliers
$74.00/200mg