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ChemicalBook CAS DataBase List 3-(TRICHLOROSTANNYL)METHYLPROPANOATE

3-(TRICHLOROSTANNYL)METHYLPROPANOATE synthesis

1synthesis methods
-

Yield:10175-01-6 98-99

Reaction Conditions:

in diethyl ether;reaction of tin, CH3OCOCH=CH2 and dry HCl in ethyl ether, product mixt extd. by warm CHCl3; purifn. of monoester by fractional recrystn.;

References:

Cheng, Hong-Shing;Hwang, Tsai-Lih;Liu, Chao-Shiuan [Journal of Organometallic Chemistry,1983,vol. 254,# 1,p. 43 - 52]